2.1 Materials:
The materials studied in this work were unidirectional carbon/epoxy composite plates made by filament winding according to the international standard ISO 1268-5 [26]. Two plates of dimensions 100 x 100 mm, with different curing cycles were considered (Table1). The curing cycle of sample 2 is recommended by the manufacturer, and that of sample 1 was chosen to have a lower Tg. They were composed of 12 layers with a thickness of approximately 0.33 mm each. T700SC-24000-50C carbon fibers were used with Araldite 1564 epoxy resin. Aradur 3474 hardener was used as a curing agent. The fiber content of the composites was 70% by mass and 60% by volume. In addition, raw matrix plates were manufactured by molding following the same curing cycles as the composites. 2017A aluminum plate was also considered as reference material for the study of thermal effects on the residual stresses.
Table 1 : Curing cycles of the samples
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Curing cycle
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Sample 1
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10 hours at 70°C
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Sample 2
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1 hour at 80°C then 4 hours at 120°C
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2.2 Methods:
As indicated in the introduction, the IHD method consists of drilling a small hole incrementally through the thickness of the material and measuring the relaxation strains for each increment. For composite materials, these strains are converted to residual stresses using the calibration coefficient matrix (equation 1):

[ε] represents the relaxation strains that are experimentally measured by IHD. [C] is the calibration coefficient matrix that is numerically calculated by the finite element method and used to convert the relaxation strains to residual stresses [19, 27]. The calculation of the residual stresses taking the incremental approach into account is given in equation 2 (Fig. 1) and a more complete description is exposed in [27].
The composite laminates were fixed on the sample holder with 4 glue points on their lower surfaces away from the hole location (more than 50 mm). The edges of the laminates were free. EA-06-062RE-120 strain gage rosettes, designed by Micro-Measurements, were glued to the samples surfaces with gage 1 aligned with the fiber direction. A National Instruments NI 9235 quarter-bridge strain gage module was used to perform the acquisition. A solid carbide milling cutter with a diameter of 2 mm and double-edged face gearing, specially designed for fiber-reinforced composites, was used. In order to study the thermal effects on residual stresses, two increment depths were considered: a large increment depth equal to 0.33 mm (1 increment per ply) and a small increment depth equal to 0.055 mm (6 increments per ply). In addition, IHD was performed on the 2017A aluminum sample, with both increment depths, to compare the influence of the increment depths to that observed on the studied composites (the calculation method has been adapted to an isotropic material [28]).
The spindle trajectories were programmed in such a way that a complete drilling cycle can be described in 5 steps.
- Rapid approach of the milling cutter: from the start position, the milling cutter descends with a speed of 1 mm/s until it reaches 85% of the current depth of the hole (depth obtained after the previous increment).
- Slow approach of the milling cutter: from 85% of the current depth, the feed speed of the milling cutter is slowed down to 0.01 mm/s.
- Drilling step: the increment is drilled with a feed speed of 0.01 mm/s.
- Rapid withdrawal: after the drilling, the milling cutter gets back to the start position with a speed of 1 mm/s.
- Relaxation: for the composite samples, a relaxation time of 90 seconds is observed for the small increment depth and 450 seconds for the large increment depth. For the aluminum sample, a relaxation time of 90 seconds is observed for both increment depths.
The rotation speed and the feed rate used are based on the work of Sicot et al.[29] . All the experimental parameters and conditions are summarized in table 2.
Table 2: Experimental parameters of the IHD tests
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Test name
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Increment depths
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Rotation speed
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Feed rate
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Ambient temperature
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Ambient humidity
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Test 0.33
Test 0.055 |
0.33 mm
0.055 mm
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5000 rpm
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0.01 mm/s
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22 ± 2 °C
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46 ± 2%
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An infrared camera (ThermaCam SC3000 designed by FLIR) was used to characterize the thermal field during and after the drilling. The thermal tests were performed at an ambient temperature of 22 ± 2 °C, without convective heat flux and isolated from any light source. ThermaCAM Researcher Professional 2.8 SR-2 software was used to post-process the results.
To better investigate the effects of drilling-induced mechanisms on the chemical properties of the samples, modulated Differential Scanning Calorimetry (DSC) tests were performed. A Discovery DSC 25 instrument designed by TA instruments was used with a ramp of 3° /min, a maximum temperature of 250 °C and a modulated temperature of 1° for 60 seconds. Two types of specimens were manually extracted from the raw matrix plates: a cold-extracted specimen and a specimen extracted after drilling on the edge of the hole.